This textbook offers a unique compendium of measurement procedures for experimental data acquisition. After introducing readers to the basic theory of uncertainty evaluation in measurements, it shows how to apply it in practice to conduct a range of laboratory experiments with instruments and procedures operating both in the time and frequency domains. Offering extensive practical information and hands-on tips on using oscilloscopes, spectrum analyzers and reflectometric instrumentation, the book shows readers how to deal with e.g. filter characterization, operational amplifiers, digital and analogic spectral analysis, and reflectometry-based measurements. For each experiment, it describes the corresponding uncertainty evaluation in detail. Bridging the gap between theory and practice, the book offers a unique, self-contained guide for engineering students and professionals alike. It also provides university teachers and professors with a valuable resource for their laboratory courses on electric and electronic measurements.