This laboratory manual offers a broad introduction to practical instrumental analysis. The practical activities include experiments for thin layer chromatography, paper chromatography, gas chromatography, high-performance liquid chromatography, electrophoresis, potentiometry, voltammetry, conductometry, coulometry, and electrogravimetry. Practical Chemistry in 3 Volumes: Volume 2: Practical Chemistry: Transition Metals, ISBN 978-3-11-157384-7 Volume 3: Practical Chemistry: Instrumental Analysis and Quantitative Analytical Chemistry, ISBN 978-3-11-170221-6