This laboratory manual offers a broad introduction to practical instrumental analysis and quantitative analytical chemistry. The practical activities include experiments to determine the quantity of analytes. Analytical techniques covered in the book are: turbidimetry, atomic absorption spectrometry, flame emission spectrometry, refractometry, infrared spectroscopy, fluorometry and UV-visible spectrophotometry. Practical Chemistry in 3 Volumes: Volume 1: Practical Chemistry: Instrumental Analysis, ISBN 978-3-11-157504-9 Volume 2: Practical Chemistry: Transition Metals, ISBN 978-3-11-157384-7